November 22, 2024
Hossein Nikmanesh

Hossein Nikmanesh

Academic Rank: Assistant professor
Address:
Degree: Ph.D in Physics
Phone: -
Faculty: Faculty of Nano and Biotechnology

Research

Title
Simultaneous substitution of chromium and zinc cations in the structure of cobalt ferrite and Nickel and investigation of their structural and magnetic properties
Type Thesis
Keywords
خواص مغناطيسي، فريت كبالت ، فريت نيكل ، جايگزيني كروم-روي، توزيع كاتيون
Researchers nahid alavi (Student) , Mahmood Niad (Primary advisor) , Hossein Nikmanesh (Primary advisor)

Abstract

Background: Spinel ferrites, MFe2O4 (M: Co, Ni, Mg, Cr, Zn, Fe) are important materials that make them suitable for various industries, biomedical and environmental applications. Among the various spinels, cobalt ferrite has attracted a lot of attention due to its remarkable properties such as high coercion field, good mechanical hardness, chemical stability, suitable saturation magnetization (Ms), crystalline magnetism, and high magnetic contraction. Aim: Investigation of changes in absorption, structural and magnetic properties with simultaneous deposition of chromium and zinc cations in cobalt ferrite and nickel ferrite structure. Methodology: In this study, structural and magnetic properties of cobalt ferrite and nickel ferrite doped by zinc and chromium (Zn_Cr) , ZnxFe2-xCrxO4Co1-x and ZnxFe2-xCrxO4Ni1-x ( X=0, 0.5, 0.75, 1) have been studied. These materials synthesized by the self-combustion sol-gel method. The iron nitrate, cobalt nitrate, nickel nitrate, zinc nitrate, chromium nitrate, and polyvinyl alcohol were selected as raw materials. The ferrite and nickel nanoparticles were identified by X-ray diffraction (XRD) by Rithold refinement through MAUD program and FTIR spectrum. A vibrating-sample magnetometer (VSM) was used to determine the magnetism of the samples. The saturated magnetism (MS) of the nano-samples that have been evaluated showed that this behavior was related to the distribution of cations in quadrilateral and octagonal holes of spinel structure by injecting Zn_Cr reducing the behavior from 27.02 emu/g to 0.5 emu/g. The evaluated coercive field (HC) reached the maximum value at X=0.5 and then decreased dramatically due to the reduction of crystalline magnetism anisotropy as a result of non-magnetic zinc ion replacement. Conclusions: It is possible to prepare cobalt ferrite as well as nickel ferrite with Zn_Cr. By replacing Co2+ and Fe3+, the size of nanoparticles increases with the exchange of Zn2+ and Cr3+, with Ni2+ and Fe3+, which can be