ONE-POT TANDEM SYNTHESIS OF b-TRIMETHYLSILYLOXY THIOESTERS FROM THIOACIDS, EPOXIDES, AND HMDS CATALYZED BY SILICA GEL UNDER SOLVENT-FREE CONDITIONS, By Mohammad Abbasi

Research

Title	ONE-POT TANDEM SYNTHESIS OF b-TRIMETHYLSILYLOXY THIOESTERS FROM THIOACIDS, EPOXIDES, AND HMDS CATALYZED BY SILICA GEL UNDER SOLVENT-FREE CONDITIONS
Type	Article
Keywords	—
Journal	SYNTHETIC COMMUNICATIONS
DOI	—
Researchers	Mohammad Abbasi (First researcher)

Abstract

a procedure for one-pot preparation of b-trimethylsilyloxy thioesters from epoxides, thioacids, and hexamethyl disilazane (HMDS) in the presence of silica gel under solvent-free condition was developed. The desired silylated products were isolated in good to excellent yields after silica-gel column chromatography.