An eco-feasible approach to synthesize of MIl 125(Ti) by using of the solvothermal process is presented in the present study. A set of characterization tests comprising X-ray Diffraction (XRD) and scanning electron microscopy (SEM) was conducted to comprehend the properties of the synthesized metal organic framework (MOF). According to the results, the applied possesses illustrate a great protentional for the synthesis of MIl 125(Ti) with a novel properties and could be proposed as a promising procedure for its large scale production and application.