مشخصات پژوهش

خانه /Design and characterization ...
عنوان
Design and characterization of nano-silica-bonded 3-n-propyl-1-sulfonic acid imidazolium chloride {nano-SB-[PSIM]Cl} as a novel, heterogeneous and reusable catalyst for the condensation of arylaldehydes with β-naphthol and alkyl carbamates
نوع پژوهش مقالات در نشریات
کلیدواژه‌ها
Nano-silica-bonded 3-n-propyl-1-sulfonic acid imidazolium chloride {nano-SB-[PSIM]Cl}; Silica-supported Brønsted acidic ionic liquid; Arylaldehyde; 2-Naphthol; Carbamatoalkyl naphthol
چکیده
In this research, nano-silica-bonded 3-n-propyl-1-sulfonic acid imidazolium chloride {nano-SB-[PSIM]Cl} as a new and efficient Brønsted acidic ionic liquid supported on silica has been synthesized, and characterized using Fourier transform infrared spectroscopy, scanning electron microscopy, transmission electron microscopy, thermogravimetric, differential thermal gravimetric, X-ray diffraction, and energy-dispersive X-ray spectroscopy spectra. The presented silica-supported ionic liquid has been applied as a highly effective, heterogeneous, easy regenerable, and reusable catalytic system for the solvent-free condensation of arylaldehydes with b-naphthol and alkyl carbamates leading to a-carbamatoalkyl-b-naphthols. Once the nanocatalyst was regenerated and reused, no significant loss of its activity was observed.
پژوهشگران عبدالکریم زارع (نفر اول)، ماریا معراج الدین (نفر دوم)، احمد رضا موسوی زارع (نفر سوم)، محمود زارعی (نفر چهارم)، محمد حسن بیضاوی (نفر پنجم)، محمد علی زلفی گل (نفر ششم به بعد)