مشخصات پژوهش

خانه /Synthesis of ...
عنوان
Synthesis of hexahydroquinolines using the new ionic liquid sulfonic acid functionalized pyridinium chloride as a catalyst
نوع پژوهش مقالات در نشریات
کلیدواژه‌ها
Brönsted acidic ionic liquid; Sulfonic acid functionalized pyridinium chloride [Pyridine‐SO3H]Cl; Hexahydroquinoline; Solvent‐free synthesis
چکیده
Sulfonic acid functionalized pyridinium chloride [pyridine-SO3H]Cl has been synthesized as a novel Brönsted acidic ionic liquid and characterized on the basis of its FT-IR, 1H and 13C NMR, MS, thermogravimetry, and derivative thermogravimetry data. The material has also been used as a highly efficient, homogeneous, and reusable catalyst for the preparation of hexahydroquinolines according to the one-pot multi-component condensation of arylaldehydes, dimedone (5,5-dimethylcyclohexane-1,3-dione), β-ketoesters, and ammonium acetate under solvent-free conditions.
پژوهشگران اردشیر خزایی (نفر اول)، محمد علی زلفی گل (نفر دوم)، احمد رضا موسوی زارع (نفر سوم)، جواد افسر (نفر چهارم)، عبدالکریم زارع (نفر پنجم)، وحید خاکی زاده (نفر ششم به بعد)، محمد حسن بیضاوی (نفر ششم به بعد)