مشخصات پژوهش

خانه /Design, characterization and ...
عنوان
Design, characterization and application of silica-bonded imidazolium-sulfonic acid chloride as a novel, active and efficient nanostructured catalyst in the synthesis of hexahydroquinolines
نوع پژوهش مقالات در نشریات
کلیدواژه‌ها
Silica-bonded imidazolium-sulfonic acidchloride SBISAC); Heterogeneous catalyst; Hexahydroquinoline; Multi-component reaction
چکیده
novel nanostructured catalyst namely silica-bonded imidazolium-sulfonic acid chloride (SBISAC) wasprepared, and fully characterized by several techniques including Fourier transform infrared spectroscopy(FT-IR), X-ray diffraction (XRD), thermal gravimetric analysis (TGA), differential thermal gravimetric(DTG), scanning electron microscope (SEM), transmission electron microscopy (TEM) and energy disper-sive X-ray analysis (EDX). The nano-compound was applied as an efficient and heterogeneous catalyst inthe synthesis of hexahydroquinolines via the one-pot multi-component condensation of arylaldehydeswith dimedone (5,5-dimethylcyclohexane-1,3-dione), beta-ketoesters and ammonium acetate under mild and solvent-free conditions.
پژوهشگران احمد رضا موسوی زارع (نفر اول)، محمد علی زلفی گل (نفر دوم)، محمود زارعی (نفر سوم)، عبدالکریم زارع (نفر چهارم)، جواد افسر (نفر پنجم)