مشخصات پژوهش

خانه /Synthesis and Identification ...
عنوان
Synthesis and Identification of SO3H-functionalized Phthalimide (SFP) as an Efficient Catalyst for the Condensation of Dimedone with Arylaldehydes
نوع پژوهش مقالات در نشریات
کلیدواژه‌ها
SO3H-functionalized phthalimide (SFP), SO3H-containing solid acid, Dimedone (5,5-Dimethyl-1,3-cyclohexanedione), Arylaldehydes, 9-Aryl-1,8-dioxo-octahydroxanthene
چکیده
A SO3 H-containing solid acid namely SO3 H-functionalized phthalimide (SFP) was synthesized from phthalimide and chlorosulfonic acid, and identified by studying its FT-IR, 1 H and 13C NMR, Mass, XRD, TG and DTG spectra. Afterward, its catalytic activity was examined for the solvent-free condensation of dimedone (5,5-dimethyl-1,3-cyclohexanedione) (2 eq.) with arylaldehydes (1 eq.). The results showed that SFP is a highly efficient catalyst to promote the title reaction for the preparation of 9-aryl-1,8-dioxo-octahydroxanthenes.
پژوهشگران عبدالکریم زارع (نفر اول)، حکیمه اسوار (نفر دوم)، فاطمه زارعی (نفر سوم)، مریم خلیلی (نفر چهارم)، زهرا کردرستمی (نفر پنجم)، احمد رضا موسوی زارع (نفر ششم به بعد)، وحید خاکی زاده (نفر ششم به بعد)